these Raw data are XRD data for ploting Figure 4a and Figure 4b

Ex-situ_1.5-5.3V_10mAg-1_5-60-117mins-Mo-60rpmRot_a_001
Expaination: 2nd Charged to 5.3V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 117 mins; Source: Mo

Ex-situ_1.5-5V_10mAg-1_5-60-117mins-Mo-60rpmRot_001
Expaination: 2nd Charged to 5V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 117 mins; Source: Mo

Ex-situ_5-1.5V_10mAg-1_5-60-117mins-Mo-60rpmRot_001
Expaination: Charged to 5V and then discharge to 1.5V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 117 mins; Source: Mo

Ex-situ_5-1.5V_10mAg-1_5-60-117mins-Mo-60rpmRot_001
Expaination: Charged to 5V and then discharge to 1.5V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 117 mins; Source: Mo

Ex-situ_5-2V_10mAg-1_5-60-117mins-Mo-60rpmRot_001
Expaination: Charged to 5V and then discharge to 2V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 117 mins; Source: Mo

Ex-situ_5-3V_10mAg-1_spin_10mm-mask_1p4mm-IS_5-60_1h_2-Theta
Expaination: Charged to 5V and then discharge to 3V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 60 mins; Source: Mo

Ex-situ_5-4V_10mAg-1_spin_10mm-mask_1p4mm-IS_5-60_1h_2-Theta
Expaination: Charged to 5V and then discharge to 4V at 10 mA/g current rate; 2 theta range: 5 to 60; Scan time: 60 mins; Source: Mo